BP305P. PHARMACEUTICAL ORGANIC CHEMISTRY -II (Practical)

Categories: 3rd Semester

Course Content

I. Experiments involving laboratory techniques
Recrystallization Steam distillation

Determination of following oil values (including standardization of reagents)
Acid value Saponification value Iodine value

Preparation of compounds
Benzanilide/Phenyl benzoate/Acetanilide from Aniline/ Phenol /Aniline by acylation reaction. 2,4,6-Tribromo aniline/Para bromo acetanilide from Aniline/ Acetanilide by halogenation (Bromination) reaction. 5-Nitro salicylic acid/Meta di nitro benzene from Salicylic acid / Nitro benzene by nitration reaction. Benzoic acid from Benzyl chloride by oxidation reaction. Benzoic acid/ Salicylic acid from alkyl benzoate/ alkyl salicylate by hydrolysis reaction. 1-Phenyl azo-2-napthol from Aniline by diazotization and coupling reactions. Benzil from Benzoin by oxidation reaction. Dibenzal acetone from Benzaldehyde by Claison Schmidt reaction Cinnammic acid from Benzaldehyde by Perkin reaction P-Iodo benzoic acid from P-amino benzoic acid

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