pharmaceutical analysis | Raghu College Of Pharmacy

About Course

Scope: This course deals with the fundamentals of analytical chemistry and principles of
electrochemical analysis of drugs

Objectives: Upon completion of the course student shall be able to
understand the principles of volumetric and electro chemical analysis  carryout various volumetric and electrochemical titrations  develop analytical skills

Course Content

pharmaceutical analysis 10 hours

– Definition and scop different techniques of analysis

00:00
Methods of expressing concentration.

00:00
Primary and secondary standards.

00:00
Preparation and standardization of various molar and normal solutions- Oxalic acid, sodium hydroxide,

00:00
Preparation and standardization of various molar and normal solutions -sodium thiosulphate and sulphuric acid,

00:00
Preparation and standardization of various molar and normal solutions potassium permanganate and ceric ammonium sulphate

00:00
Errors: Sources of errors, types of errors, methods of minimizing errors,

00:00
methods of minimizing errors

00:00
accuracy, precision and significant figures

00:00
Pharmacopoeia, Sources of impurities in medicinal agents ,limit tests.

00:00

Acid base titrations-non aqueous titrations 10 hours

Acid base titration: Theories of acid base indicators,

00:00
classification of acid base titrations

00:00
Theory involved in acid – base titrations

00:00
Theory involved in titrations of strong ,week and very week acids and bases

00:00
neutralization curves-

00:00
Tutorial over-

00:00
Non aqueous titration: Solvents and classification

00:00
Non aqueous titration: Acidemetry and Alkalimetry titration-

00:00
Estimation of Sodium benzoate and Ephedrine HCl-

00:00
Tutorial over-

00:00

Precipitation titrations-complexometric titrations- gravimetry 10 hours

Precipitation titrations: Mohr’s method, Volhard’s-

00:00
Precipitation titrations: Modified Volhard’s, Fajans method, –

00:00
Precipitation titrations: estimation of sodium chloride.

00:00
Complexometric titration: Classification, metal ion indicators-

00:00
Complexometric titration: masking and demasking reagents-

00:00
Complexometric titration: calcium gluconate

00:00
Gravimetry: Principle and steps involved in gravimetric analysis-

00:00
Purity of the precipitate: co-precipitation and post precipitation-

00:00
Gravimetry: Principle and steps involved in Estimation of barium sulphate.-

00:00
Basic Principles, methods and application of diazotisation titration

00:00

redox titrations 08 hours

electrochemical methods of analysis 07 hours

Conductometry- Introduction, Conductivity cell-

00:00
Conductometry- Conductometric titrations, applications-

00:00
Electrochemical cell, construction and working of reference (Standard hydrogen)

00:00
– Electrochemical cell, construction and working of reference( silver chloride electrode ,calomel electrode)

00:00
indicator electrodes (metal electrodes and glass electrode)-

00:00
, methods to determine end point of potentiometric titration and applications-

00:00
Polarography – Principle, Ilkovic equation, construction –

00:00
working of dropping mercury electrode and rotating platinum electrode, applications-

00:00

Student Ratings & Reviews

5.0

Total 2 Ratings

2 Ratings

0 Rating

KONA PADMA RAMALAKSHMI

2 years ago

Excellent

KILARI SRI VYSHNAVI

2 years ago

It is very understansable. Video are also available in this course which is very useful.

About Course

Course Content

pharmaceutical analysis 10 hours

– Definition and scop different techniques of analysis

Methods of expressing concentration.

Primary and secondary standards.

Preparation and standardization of various molar and normal solutions- Oxalic acid, sodium hydroxide,

Preparation and standardization of various molar and normal solutions -sodium thiosulphate and sulphuric acid,

Preparation and standardization of various molar and normal solutions potassium permanganate and ceric ammonium sulphate

Errors: Sources of errors, types of errors, methods of minimizing errors,

methods of minimizing errors

accuracy, precision and significant figures

Pharmacopoeia, Sources of impurities in medicinal agents ,limit tests.

Acid base titrations-non aqueous titrations 10 hours

Acid base titration: Theories of acid base indicators,

classification of acid base titrations

Theory involved in acid – base titrations

Theory involved in titrations of strong ,week and very week acids and bases

neutralization curves-

Tutorial over-

Non aqueous titration: Solvents and classification

Non aqueous titration: Acidemetry and Alkalimetry titration-

Estimation of Sodium benzoate and Ephedrine HCl-

Tutorial over-

Precipitation titrations-complexometric titrations- gravimetry 10 hours

Precipitation titrations: Mohr’s method, Volhard’s-

Precipitation titrations: Modified Volhard’s, Fajans method, –

Precipitation titrations: estimation of sodium chloride.

Complexometric titration: Classification, metal ion indicators-

Complexometric titration: masking and demasking reagents-

Complexometric titration: calcium gluconate

Gravimetry: Principle and steps involved in gravimetric analysis-

Purity of the precipitate: co-precipitation and post precipitation-

Gravimetry: Principle and steps involved in Estimation of barium sulphate.-

Basic Principles, methods and application of diazotisation titration

redox titrations 08 hours

Concepts of oxidation and reduction –

Types of redox titrations (Principles and applications) –

Principles and applications Cerimetry, Iodimetry, –

Principles and applications Iodimetry, Iodometry, –

Principles and applications: Bromatometry,

Principles and applications: Dichrometry,-

Principles and applications : Titration with potassium iodate

Tutorial over-

electrochemical methods of analysis 07 hours

Conductometry- Introduction, Conductivity cell-

Conductometry- Conductometric titrations, applications-

Electrochemical cell, construction and working of reference (Standard hydrogen)

– Electrochemical cell, construction and working of reference( silver chloride electrode ,calomel electrode)

indicator electrodes (metal electrodes and glass electrode)-

, methods to determine end point of potentiometric titration and applications-

Polarography – Principle, Ilkovic equation, construction –

working of dropping mercury electrode and rotating platinum electrode, applications-

Student Ratings & Reviews