X-Ray Diffraction Methods: Origin of X-rays | Raghu College Of Pharmacy

Course Content

Nuclear Magnetic Resonance spectroscopy

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Principles of H-NMR and C-NMR

factors affecting chemical shift

coupling constant, Spin – spin coupling, relaxation

instrumentation and applications

Mass Spectrometry

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Ionization techniques – Electron impact, chemical ionization

Analyzers-Time of flight and Quadrupole,

instrumentation, applications

Unit – 3: Calibration -as per ICH and USFDA guidelines

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Calibration -as per ICH and USFDA guidelines Validation-as per ICH and USFDA guidelines

Calibration of UV-Visible spectrophotometer

Calibration of IR spectrophotometer,

Calibration of Electronic balance

Calibration of Fluorimeter

Calibration of Flame Photometer

Calibration of HPLC

Calibration of GC

Unit – 2: Thermal Methods of Analysis

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Principles of TGA

Instrumentation of ThermogravimetricAnalysis (TGA)

Applications of ThermogravimetricAnalysis (TGA)

Differential Thermal Analysis (DTA),

Differential Scanning Calorimetry (DSC)

X-Ray Diffraction Methods: Origin of X-rays

basic aspects of crystals,

X- ray Crystallography

Rotating crystal technique, single crystal diffraction,

powder, Diffraction

BP 811 ET. ADVANCED INSTRUMENTATION TECHNIQUES- 45 Hours

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